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Creators/Authors contains: "Brisset, François"

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  1. The static recrystallization and grain growth of a hybrid AZ31/Mg-0.6Gd (wt%) material fabricated by high pressure torsion (HPT) through 20 turns were explored after isochronal annealing at 150, 250, 350 and 450 ◦C for 1 h using electron backscatter diffraction, transmission electron microscopy and Vickers microhardness measurements. The results reveal heterogeneity in the grain size distributions of the AZ31 and Mg-0.6Gd regions after annealing at the lower temperatures of 150 and 250 ◦C leading to a clear AZ31/Mg-0.6Gd interfacial border. At the higher temperatures of 350 and 450 ◦C the AZ31/Mg-0.6Gd interfaces were not well-defined owing to the occurrence of grain growth. It is shown that grain growth is restricted in the AZ31 and Mg-0.6Gd regions due to the presence of stable nano-size Al8Mn5 particles and the precipitation of Mg17Al12 and Mg12Zn at 250 ◦C and of Mg5Gd and Mg12Gd phases at 350 and 450 ◦C. The distribution of the basal texture in both regions was strongly controlled by dynamic recrystallization, precipitation and grain growth. The values of the microhardness over the radial cross-sections of the hybrid discs decrease and become more uniform, in the range of ~35–66 Hv, with increasing annealing temperature. 
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    Free, publicly-accessible full text available February 5, 2026
  2. null (Ed.)